STOE IPDS 1 diffractometer | 4545 independent reflections |
Radiation source: fine-focus sealed tube | 3172 reflections with I > 2σ(I) |
Plane graphite monochromator | Rint = 0.091 |
φ rotation scans | θmax = 25.9°, θmin = 2.3° |
Absorption correction: multi-scan (MULABS; Spek, 2009) | h = −18→18 |
Tmin = 0.712, Tmax = 1.000 | k = −13→13 |
18018 measured reflections | l = −18→18 |