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. 2017 Sep 8;73(Pt 10):1421–1425. doi: 10.1107/S2056989017012543
STOE IPDS 1 diffractometer 4545 independent reflections
Radiation source: fine-focus sealed tube 3172 reflections with I > 2σ(I)
Plane graphite monochromator Rint = 0.091
φ rotation scans θmax = 25.9°, θmin = 2.3°
Absorption correction: multi-scan (MULABS; Spek, 2009) h = −18→18
Tmin = 0.712, Tmax = 1.000 k = −13→13
18018 measured reflections l = −18→18