Table 2. Experimental details.
| Crystal data | |
| Chemical formula | C32H40NO2·C7H3N2O6 |
| M r | 681.76 |
| Crystal system, space group | Monoclinic, P21/c |
| Temperature (K) | 293 |
| a, b, c (Å) | 5.9168 (3), 28.3733 (12), 21.0782 (11) |
| β (°) | 97.836 (5) |
| V (Å3) | 3505.6 (3) |
| Z | 4 |
| Radiation type | Mo Kα |
| μ (mm−1) | 0.09 |
| Crystal size (mm) | 0.23 × 0.21 × 0.18 |
| Data collection | |
| Diffractometer | Rigaku Saturn724 |
| Absorption correction | Multi-scan (SADABS; Krause et al., 2015 ▸) |
| T min, T max | 0.956, 0.984 |
| No. of measured, independent and observed [I > 2σ(I)] reflections | 40112, 7331, 4388 |
| R int | 0.061 |
| (sin θ/λ)max (Å−1) | 0.629 |
| Refinement | |
| R[F 2 > 2σ(F 2)], wR(F 2), S | 0.065, 0.179, 1.05 |
| No. of reflections | 7331 |
| No. of parameters | 470 |
| No. of restraints | 22 |
| H-atom treatment | H atoms treated by a mixture of independent and constrained refinement |
| Δρmax, Δρmin (e Å−3) | 0.20, −0.25 |