| Rigaku R-AXIS RAPIDII diffractometer | 4124 reflections with I > 2σ(I) |
| Detector resolution: 10.000 pixels mm-1 | Rint = 0.036 |
| ω scans | θmax = 30.0°, θmin = 3.0° |
| Absorption correction: numerical (NUMABS; Higashi, 1999) | h = −7→7 |
| Tmin = 0.890, Tmax = 0.948 | k = −11→11 |
| 12373 measured reflections | l = −25→25 |
| 4597 independent reflections |
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