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. 2017 Dec 20;7:17934. doi: 10.1038/s41598-017-18109-z

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© The Author(s) 2017

Open Access This article is licensed under a Creative Commons Attribution 4.0 International License, which permits use, sharing, adaptation, distribution and reproduction in any medium or format, as long as you give appropriate credit to the original author(s) and the source, provide a link to the Creative Commons license, and indicate if changes were made. The images or other third party material in this article are included in the article’s Creative Commons license, unless indicated otherwise in a credit line to the material. If material is not included in the article’s Creative Commons license and your intended use is not permitted by statutory regulation or exceeds the permitted use, you will need to obtain permission directly from the copyright holder. To view a copy of this license, visit http://creativecommons.org/licenses/by/4.0/.

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2D ¹H-¹⁵N CP-HSQC SSNMR spectrum of ANSII-GNPs (black) superimposed with the spectrum of crystalline ANSII (red) (panel A), and PEG-ANSII (blue) (panel B). The superimposition of the spectra of crystalline and PEG-ANSII is also reported (panel C). The spectrum of ANSII-GNPs was acquired on a 800 MHz spectrometer, while the spectra of crystalline ANSII and PEG-ANSII were acquired on a 850 MHz spectrometer. All the spectra were recorded at ~282 K and MAS of 60 kHz.