Table 1. The basic information of the five principal components.
Peak no. | Retention time (min) | Chemical structure | Chemical name |
---|---|---|---|
1 | 6.654 | R1 = Tig, R2 = Ac | Tenacissoside G [18] |
2 | 7.475 | R1 = Bz, R2 = Ac | Tenacissoside I [18] |
3 | 12.258 | R1 = Bu, R2 = Tig | Marsdenoside A [19] |
4 | 14.455 | R1 = Tig, R2 = Tig | Marsdenoside B [19] |
5 | 15.937 | R1 = Bu, R2 = Bz | Marsdenoside C [19] |
Five compounds 1∼5 were isolated from FR5 by preparative high performance liquid chromatography (HPLC) and identified by nuclear magnetic resonance (NMR) analyses and compared with the literatures.