Table 4.
Data collection, phasing and refinement statistics of 5MVL (MAD)
| 5MVL | ||
|---|---|---|
| Data collection | ||
| Space group | P3221 | |
| Cell dimensions | ||
| a, b, c (Å) | 43.5, 43.5, 60.8 | |
| α, β, γ(°) | 90.0, 90.0, 120.0 | |
| Peak | Remote | |
|
|
||
| Wavelength | 0.920 | 1.240 |
| Resolution (Å)a | 30.4-1.6 (1.63-1.6)a | 30.4-1.4 (1.43-1.40) |
| Rmeas | 5.5 (52.9) | 4.6 (117) |
| I/σ(I) | 18.8 (4.1) | 23.4 (2.0) |
| CC1/2 | 0.999 (0.898) | 0.999 (0.984) |
| Completeness (%) | 99.1 (100) | 99.9 (100) |
| Redundancy | 7.9 (8.0) | 9.1 (8.3) |
| Refinement | ||
| Resolution (Å) | 23.7-1.4 | |
| No. reflections | 13,446 | |
| Rwork / Rfree | 15.7 / 18.2 | |
| No. atoms | ||
| DNA | 486 | |
| Mg2+ | 1 | |
| Water | 76 | |
| B factors | ||
| DNA | 23.89 | |
| Water | 33.90 | |
| R.m.s deviations | ||
| Bond lengths (Å) | 0.009 | |
| Bond angles (°) | 1.07 | |
Both data sets were collected from a single crystal.
a
Values in parentheses are for highest-resolution shell.