Table 2.
entry | R1 | R2 | yield (step 2, %) |
1 | iBu | Cbz | 77 |
2 | iBu | P(O)(OPh)2 | 84 |
3 | iBu | t-BuSO2 | 81 |
4 | iBu | Ns | 54 |
5 | iPr | Cbz | 76 |
6 | Ph | t-BuSO2 | 76 |
7 | Ph | 83 |
entry | R1 | R2 | yield (step 2, %) |
1 | iBu | Cbz | 77 |
2 | iBu | P(O)(OPh)2 | 84 |
3 | iBu | t-BuSO2 | 81 |
4 | iBu | Ns | 54 |
5 | iPr | Cbz | 76 |
6 | Ph | t-BuSO2 | 76 |
7 | Ph | 83 |