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. 2018 Jan 9;9:108. doi: 10.1038/s41467-017-02575-0

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© The Author(s) 2017

Open Access This article is licensed under a Creative Commons Attribution 4.0 International License, which permits use, sharing, adaptation, distribution and reproduction in any medium or format, as long as you give appropriate credit to the original author(s) and the source, provide a link to the Creative Commons license, and indicate if changes were made. The images or other third party material in this article are included in the article’s Creative Commons license, unless indicated otherwise in a credit line to the material. If material is not included in the article’s Creative Commons license and your intended use is not permitted by statutory regulation or exceeds the permitted use, you will need to obtain permission directly from the copyright holder. To view a copy of this license, visit http://creativecommons.org/licenses/by/4.0/.

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Fig. 6 — Sub-picomole detection combining photo-CIDNP and microcoil NMR technology. Top: ¹⁹F NMR spectrum of a sample containing 0.4 mM of p-fluorophenol, which cannot be detected. Bottom of figure: The photo-CIDNP spectrum under flow conditions of a 0.8 μM p-fluorophenol sample. This corresponds to detection of just 0.8 picomole of material per μL. The number of accumulated scans is 14 in both cases