Table 6.
Robustness test results.
| Parameters | Polyoxyl 15 hydroxystearate |
Caprylic acid triglyceride |
Capric acid triglyceride |
|||||||||||||
|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|
| Peak area | Diff. (%) | Peak area | Diff. (%) | Peak area | Diff. (%) | |||||||||||
| Flow rate (mL/min) | ||||||||||||||||
| 0.7 | 1,459,980 | 611,306 | 607,004 | |||||||||||||
| 0.6 | 1,499,094 | 2.68 | 535,450 | −12.41 | 617,440 | 1.72 | ||||||||||
| Column temperature (°C) | ||||||||||||||||
| 30 | 1,183,531 | 557,103 | 498,911 | |||||||||||||
| 45 | 1,174,089 | −0.80 | 554,693 | −0.43 | 483,495 | −3.09 | ||||||||||
| Evaporation temperature in NQAD (°C) | ||||||||||||||||
| 45 | 1,313,528 | 451,385 | 456,791 | |||||||||||||
| 60 | 1,307,247 | −0.48 | 449,095 | −0.51 | 464,495 | 1.69 | ||||||||||
| Nebulization temperature in NQAD (°C) | ||||||||||||||||
| 35 | 1,307,247 | 449,895 | 463,749 | |||||||||||||
| 40 | 1,295,625 | −0.89 | 463,539 | 3.03 | 474,011 | 2.21 | ||||||||||