| Stoe IPDS 2 diffractometer | 2776 independent reflections |
| Radiation source: sealed X-ray tube, 12 x 0.4 mm long-fine focus | 2011 reflections with I > 2σ(I) |
| Plane graphite monochromator | Rint = 0.109 |
| Detector resolution: 6.67 pixels mm-1 | θmax = 26.0°, θmin = 2.6° |
| rotation method scans | h = −8→8 |
| Absorption correction: integration (X-RED32; Stoe & Cie, 2002) | k = −9→9 |
| Tmin = 0.947, Tmax = 0.972 | l = −19→19 |
| 10204 measured reflections |
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