Table 2. Experimental details.
| Crystal data | |
| Chemical formula | C17H13NO2 |
| M r | 263.28 |
| Crystal system, space group | Monoclinic, P21/c |
| Temperature (K) | 100 |
| a, b, c (Å) | 15.353 (3), 6.3143 (13), 26.941 (6) |
| β (°) | 96.446 (4) |
| V (Å3) | 2595.3 (9) |
| Z | 8 |
| Radiation type | Mo Kα |
| μ (mm−1) | 0.09 |
| Crystal size (mm) | 0.43 × 0.14 × 0.06 |
| Data collection | |
| Diffractometer | Bruker SMART APEX CCD |
| Absorption correction | Multi-scan (SADABS; Bruker, 2003 ▸) |
| T min, T max | 0.707, 0.995 |
| No. of measured, independent and observed [I > 2σ(I)] reflections | 21411, 5293, 3646 |
| R int | 0.089 |
| (sin θ/λ)max (Å−1) | 0.625 |
| Refinement | |
| R[F 2 > 2σ(F 2)], wR(F 2), S | 0.080, 0.147, 1.11 |
| No. of reflections | 5293 |
| No. of parameters | 369 |
| H-atom treatment | H atoms treated by a mixture of independent and constrained refinement |
| Δρmax, Δρmin (e Å−3) | 0.25, −0.30 |