Table 1. Hydrogen-bond geometry (Å, °).
| D—H⋯A | D—H | H⋯A | D⋯A | D—H⋯A |
|---|---|---|---|---|
| N1A—H1NA⋯O6A | 0.86 (3) | 2.40 (3) | 2.813 (3) | 110 (2) |
| N1A—H1NA⋯O7A | 0.86 (3) | 2.30 (3) | 2.674 (2) | 107 (2) |
| O2B—H2OB⋯O8A i | 0.84 (3) | 1.78 (3) | 2.596 (3) | 165 (3) |
| N1A—H2NA⋯O7B | 0.98 (3) | 1.78 (3) | 2.743 (3) | 169 (3) |
| O5A—H5OA⋯O2B ii | 0.76 (4) | 2.14 (4) | 2.886 (3) | 168 (4) |
| O5B—H5OB⋯O3A iii | 0.83 (4) | 1.99 (4) | 2.804 (3) | 165 (3) |
| O2A—H2OA⋯O3A | 0.82 (4) | 2.62 (3) | 2.847 (2) | 97 (3) |
| O3A—H3OA⋯O4B iv | 0.78 (4) | 2.08 (4) | 2.785 (3) | 149 (3) |
| O4A—H4OA⋯O8A v | 0.84 (4) | 2.00 (4) | 2.822 (3) | 170 (4) |
| O2A—H2OA⋯O8B | 0.82 (4) | 1.87 (4) | 2.657 (3) | 161 (4) |
| O4B—H4OB⋯O3B | 0.84 (4) | 2.51 (4) | 2.886 (2) | 108 (3) |
| O4B—H4OB⋯O4A vi | 0.84 (5) | 2.14 (5) | 2.864 (3) | 145 (5) |
| N1B—H2NB⋯O7A i | 0.90 (3) | 1.91 (3) | 2.795 (3) | 168 (3) |
| N1B—H1NB⋯O3B | 0.90 (4) | 2.02 (4) | 2.800 (3) | 144 (3) |
| N1B—H1NB⋯O7B | 0.90 (4) | 2.40 (3) | 2.681 (3) | 100 (2) |
| O3B—H3OB⋯O5B vii | 0.86 (4) | 1.92 (4) | 2.717 (3) | 154 (4) |
Symmetry codes: (i)
; (ii)
; (iii)
; (iv)
; (v)
; (vi)
; (vii)
.