| Crystal data |
| Chemical formula |
C10H19NO7
|
|
M
r
|
265.26 |
| Crystal system, space group |
Triclinic, P1 |
| Temperature (K) |
100 |
|
a, b, c (Å) |
5.8008 (19), 9.636 (3), 10.676 (4) |
| α, β, γ (°) |
87.766 (3), 86.330 (4), 82.042 (4) |
|
V (Å3) |
589.5 (3) |
|
Z
|
2 |
| Radiation type |
Mo Kα |
| μ (mm−1) |
0.13 |
| Crystal size (mm) |
0.25 × 0.20 × 0.08 |
| |
| Data collection |
| Diffractometer |
Bruker APEXII CCD area detector |
| Absorption correction |
Multi-scan (SADABS; Sheldrick, 2003 ▸) |
|
T
min, T
max
|
0.86, 0.99 |
| No. of measured, independent and observed [I > 2σ(I)] reflections |
6952, 5160, 4927 |
|
R
int
|
0.022 |
| (sin θ/λ)max (Å−1) |
0.652 |
| |
| Refinement |
|
R[F
2 > 2σ(F
2)], wR(F
2), S
|
0.033, 0.081, 1.03 |
| No. of reflections |
5160 |
| No. of parameters |
377 |
| No. of restraints |
3 |
| H-atom treatment |
H atoms treated by a mixture of independent and constrained refinement |
| Δρmax, Δρmin (e Å−3) |
0.30, −0.22 |
| Absolute structure |
Flack x determined using 2254 quotients [(I
+)−(I
−)]/[(I
+)+(I
−)] (Parsons et al., 2013 ▸) |
| Absolute structure parameter |
−0.5 (3) |
