Table 1.
Case | Step 1 | Step 2 | ||||
---|---|---|---|---|---|---|
Chemicals | Conditions | Solid loading (%) | Chemicals | Conditions | Solid loading (%) | |
1 | 1% NaOH | 120 °C, 60 min | 10 | – | – | – |
2 | Liquid hot water | 120 °C, 30 min | 10 | 1% NaOH | 120 °C, 60 min | 10 |
3 | Liquid hot water | 120 °C, 30 min | 10 | 50% ethanol + 1% NaOH | 120 °C, 60 min | 10 |
4 | 1% H2SO4 | 120 °C, 30 min | 10 | 1% NaOH | 120 °C, 60 min | 10 |
5 | 1% H2SO4 | 120 °C, 30 min | 10 | 50% ethanol + 1% NaOH | 120 °C, 60 min | 10 |
% was calculated based on the weight percent, w/w