Table 1.
QC level (ng/mL) | Ergocalciferol |
Ergocalciferol-d6 |
||||
---|---|---|---|---|---|---|
Mean area response |
Extraction recovery (%) | Mean area response |
Extraction recovery (%) | |||
Post-extraction spiking | Pre-extraction spiking | Post-extraction spiking | Pre-extraction spiking | |||
HQC (80.0) | 7006545 | 5818432 | 83.0 | 493724 | 427070 | 86.5 |
MQC-1 (40.0) | 3578144 | 3001422 | 83.9 | 483473 | 419236 | 86.7 |
MQC-2 (3.00) | 287385 | 240530 | 83.7 | 493898 | 431564 | 85.4 |
LQC (0.300) | 29514 | 25201 | 85.4 | 489605 | 427845 | 87.4 |
HQC: high quality control; MQC: medium quality control; LQC: low quality control.
Extraction recovery: (pre-extraction spiking/post-extraction spiking) × 100.