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Reaction of melittin (MWcalc= 2847) with NaTFMS/TBHP. (a) Relative conversions from LC-MS with the optimal reaction time highlighted in blue. (b) Deconvoluted LC-MS spectra of reaction mixtures after 5 min ± Met. Undesired oxidation (+32) is curtailed by sacrificial reductant giving melittin-TrpCF3 (+68, MWcalc = 2915, MWfound = 2915).
