. Author manuscript; available in PMC: 2018 Feb 14.

Published in final edited form as: Biochemistry. 2008 Sep 17;47(40):10685–10693. doi: 10.1021/bi801309q

Table 1.

X-ray Data Collection Statistics.

	Enzyme Complexed with GDP-perosamine	Enzyme Complexed with GDP-3-deoxyperosamine
space group	P2₁	P2₁
unit cell dimensions (Å)	a = 50.1, b = 151.9, c = 105.7, β = 102.1°	a = 50.4, b = 152.2, c = 105.8, β = 101.8°
resolution limits	50 – 1.6 (1.66 – 1.6)^b	100 – 1.7 (1.8 – 1.7)^b
number of independent reflections	186452 (16930)	161560 (22419)
completeness (%)	91.9 (83.8)	94.6 (83.2)
redundancy	6.3 (4.6)	3.7 (1.7)
avg I/avg σ(I)	11.5 (7.6)	10.7 (2.3)
R_sym (%)^a	4.1 (21.4)	8.6 (42.4)

R_sym = (Σ|Σ I − Ī|/ΣI) × 100.

Statistics for the highest resolution bin.