Table 1. Effect of the amount of base (K2CO3) on the synthesis of 3a, 3b (Stoichiometric 2/diphenols mixture, 75 °C, 96 h).
Base amount/diphenols | 3 eq | 4 eq | 5 eq | 6 eq | 7 eq | |
---|---|---|---|---|---|---|
Yield (%) | 3a | 38 | 41 | 48 | 50 | 49 |
3b | 28 | 31 | 42 | 44 | 43 |
Base amount/diphenols | 3 eq | 4 eq | 5 eq | 6 eq | 7 eq | |
---|---|---|---|---|---|---|
Yield (%) | 3a | 38 | 41 | 48 | 50 | 49 |
3b | 28 | 31 | 42 | 44 | 43 |