Table 3. Effect of reaction time on the synthesis of 3a, 3b (Stoichiometric 2/diphenols mixture, K2CO3/diphenols molar ratio: 5, 75 °C).
Time (day) | 1 | 2 | 3 | 4 | 5 | 7 | |
---|---|---|---|---|---|---|---|
Yield (%) | 3a | 29 | 32 | 36 | 48 | 52 | 60 |
3b | 26 | 27 | 29 | 42 | 47 | 58 |
Time (day) | 1 | 2 | 3 | 4 | 5 | 7 | |
---|---|---|---|---|---|---|---|
Yield (%) | 3a | 29 | 32 | 36 | 48 | 52 | 60 |
3b | 26 | 27 | 29 | 42 | 47 | 58 |