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. 2017 Nov 13;20(1):547–563. doi: 10.1080/15685551.2017.1395502

Table 5. Obtained reaction yields of the synthesis of 3b under MW (Stoichiometric 2/THIO mixture, K2CO3/THIO molar ratio = 5).

Temperature (°C) 85 95 100
Reaction time (h) 7.5 8 7.5 8 7.5 8
Yield (%) 58 63 64 72 60 68