Table 5. Obtained reaction yields of the synthesis of 3b under MW (Stoichiometric 2/THIO mixture, K2CO3/THIO molar ratio = 5).
Temperature (°C) | 85 | 95 | 100 | |||
---|---|---|---|---|---|---|
Reaction time (h) | 7.5 | 8 | 7.5 | 8 | 7.5 | 8 |
Yield (%) | 58 | 63 | 64 | 72 | 60 | 68 |
Temperature (°C) | 85 | 95 | 100 | |||
---|---|---|---|---|---|---|
Reaction time (h) | 7.5 | 8 | 7.5 | 8 | 7.5 | 8 |
Yield (%) | 58 | 63 | 64 | 72 | 60 | 68 |