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2H static solid echo NMR spectra of (a) [D12]TCC2‐R (blue), (b) iodine‐loaded [D12]TCC2‐R (dark blue), (c) [D12]TCC3‐R (red), (d) iodine‐loaded [D12]TCC3‐R (burgundy) and their corresponding simulated spectra (black dashed lines) obtained at various temperatures. The rotational rates, k, obtained from numerical simulations of the NMR lineshapes are also given. Spectral artefacts are denoted with (#).
