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Representative chromatograms obtained from the analysis of human plasma using (a) procedure (A), PP with aqueous TCA; (b) procedure (B), PP with a mixture of acetonitrile and ammonia (90 : 10); and (c) procedure (C), SPE cleanup with Oasis MCX. Insets: zoom of the ADMA and SDMA peaks at 18.1 and 19.0 min, respectively.
