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Study of the oxidation potential during the electrolysis. a Cyclic voltammograms in CF3CH2OH (10 mL) with 0.06 M nBu4NBF4: blue line, 1a (0.050 mmol); red line, Co(acac)2 (0.050 mmol); green line, a mixture of Co(acac)2 (0.050 mmol), and 1a (0.050 mmol). b Potential controlled electrolysis at 1.13 V (vs Ag/AgCl)
