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. Author manuscript; available in PMC: 2019 Jan 10.
Published in final edited form as: J Am Chem Soc. 2017 Dec 19;140(1):22–25. doi: 10.1021/jacs.7b09744

Figure 1.

Figure 1

CVs of NHPI (1 mM) in acetonitrile (a); in the presence of pyridine/pyridinium perchlorate (0.1 M each) (b); pyridine (0.01 M) and solid KHCO3 (100 equiv) (c); and in the presence of pyridine/pyridinium perchlorate (0.1 M each), and 4-tBu-toluene (20 mM) (d). Other conditions: glassy carbon working electrode, scan rate = 10 mV/s, and 0.1 M KPF6 electrolyte for (a) and (c).