Skip to main content
. Author manuscript; available in PMC: 2019 Jan 10.
Published in final edited form as: J Am Chem Soc. 2017 Dec 19;140(1):22–25. doi: 10.1021/jacs.7b09744

Table 2.

Electrochemical iodination of methylarenes mediated by NHPI.a

graphic file with name nihms942523f6.jpg
a

A: 0.1 M 1, 20 mol% NHPI, 50 mol% I2, 0.2 M Lut/0.1 M LutH+ClO4−, 10 mL MeCN, 5 mA. B: 0.1 M substrate 1, 20 mol% NHPI, 50 mol% I2, 0.2 M 2,6-di-tBuPy, 0.1 M 2,6-di-tBuPyH+ClO4−, 10 mL MeCN, 5 mA. 1H NMR yields (isolated yields in parentheses).12