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. Author manuscript; available in PMC: 2019 Jan 10.
Published in final edited form as: J Am Chem Soc. 2017 Dec 19;140(1):22–25. doi: 10.1021/jacs.7b09744

Table 3.

In situ methylarene iodination/alkylation of pyridine under NHPI-mediated electrolysis conditions.a

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a

Conditions: 0.3 M substrate 1, 15 mol% NHPI, 20 mol% I2, 0.6 M Pyridine, 0.6 M PyH+ClO4−, 10 mL MeCN, 15 mA. 1H NMR yield (ext. std. = mesitylene). 1H NMR yields (isolated yields in parentheses).12