Selected hydrogen bond geometry parameters (Å, °) for 8.
D–H⋯A | D–H | H⋯A | D⋯A | D–H⋯A |
---|---|---|---|---|
N5–H5⋯O7a | 0.89 (6) | 2.02 (6) | 2.883 (7) | 162 (6) |
N6–H6A⋯Cl2b | 0.85 (6) | 2.56 (6) | 3.334 (6) | 152 (5) |
N6–H6B⋯O10Ba | 0.90 (7) | 2.04 (7) | 2.933 (14) | 169 (6) |
N15–H15⋯O1c | 0.81 (6) | 2.11 (6) | 2.878 (6) | 158 (5) |
N16–H16A⋯Cl2b | 0.93 (5) | 2.64 (5) | 3.367 (6) | 136 (4) |
N16–H16B⋯O5 | 0.81 (6) | 2.12 (6) | 2.910 (7) | 166 (5) |
O5–H5A⋯Cl2 | 0.99 (6) | 2.19 (6) | 3.172 (6) | 172 (5) |
N14–H14⋯O3d | 0.81 (7) | 1.97 (7) | 2.761 (5) | 164 (7) |
O5–H5B⋯O11c | 0.99 (2) | 2.50 (14) | 3.416 (9) | 154 (25) |
−x + 1, y + 1/2, −z + 3/2.
−x, −y + 1, −z + 2.
x − 1, y, z.
−x, −y + 1, −z + 1.