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. Author manuscript; available in PMC: 2018 Mar 1.
Published in final edited form as: Chemphyschem. 2016 Jul 22;17(19):2962–2966. doi: 10.1002/cphc.201600637

Figure 4.

Figure 4

1H-detected 2D 1H/13C HETCOR spectrum of danazol/vanillin co-crystals obtained using the pulse sequence shown in Figure 1c with N=1(black) and N=3(red). The initial 1H→13C CP contact time was 2.0 ms, and each 13C→1H CP contact time was 0.4 ms. Other experimental parameters include 6 ms of each signal acquisition, 7 s recycle delay, and 36 scans for each t1 increment.