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. 2018 Feb 26;8:3647. doi: 10.1038/s41598-018-21957-y

Figure 6.

Figure 6

(A) Precursor capsules were prepared by ultra-sonicating an oil phase (hexadecane, toluene diisocyanate and with or without superparamagnetic nanoparticles, SPION) with a suspension of CNF/CNC to form an oil in water emulsion. The reaction took place at the oil droplet’s interface. Precursor capsules were added to a PVP solution in EtOH (B). The suspension was washed and then dispersed in an EtOH/Water mixture and TEOS and ammonia were added (C) to form capsules with silica nanoparticles on the outer capsule walls (D). Afterwards, the hybrid capsules were further treated with fluorosilane (E).