Table 2.

Sensitivity, accuracy and precision of the developed method.

Analyte	Spiked level (ng mL−1)	Measured (ng mL−1)	Method recovery (%)	RSDr		LOD (ng mL−1)	LOQ (ng mL−1)
				Intra-day (n = 6)	Inter-day (n = 18)
DON	2	1.9	94	12.5	13.3	0.5	1
	10	11.2	112	3.8	3.2
	50	20.8	104	7.1	8.4
DOM-1	2	1.6	80	7.3	9.5	0.1	0.2
	10	9.1	91	6.4	4.5
	50	18.2	91	4.4	6.6