Table 1.
Data collection and refinement statistics
| l‐Lys complex | l‐Orn complex | l‐Arg complex | |
|---|---|---|---|
| Data collection | |||
| PDB entry | 5YB6 | 5YB7 | 5YB8 |
| Space group | P21 | P21 | P21 |
| Unit cell (Å) | a = 97.1, b = 132.3 | a = 94.6, b = 132.9 | a = 98.2, b = 133.0 |
| c = 101.0 | c = 101.9 | c = 101.5 | |
| β (°) = 108.7 | β (°) = 111.5 | β (°) = 112.0 | |
| Resolution (Å) | 50.00–2.10 (2.14–2.10) | 94.81–2.00 (2.15–2.00) | 94.11–2.30 (2.42–2.30) |
| Total reflections | 473 819 | 590 825 | 404 779 |
| Unique reflections | 139 347 | 156 339 | 106 954 |
| Completeness (%) | 99.5 (99.7) | 98.9 (98.0) | 99.7 (99.8) |
| Redundancy | 3.4 (3.3) | 3.8 (3.7) | 3.8 (3.8) |
| Mean I/σ | 10.6 (2.9) | 16.0 (3.7) | 12.0 (3.2) |
| R merge (%) | 12.6 (35.1) | 5.4 (40.7) | 8.1 (47.2) |
| Refinement | |||
| Resolution (Å) | 50.00–2.10 | 94.81–2.00 | 94.11–2.30 |
| No. of reflections | 132 300 | 144 806 | 104 920 |
| R/R free (%) | 23.7/28.3 | 19.8/24.0 | 22.0/27.3 |
| No. of atoms | 18 833 | 18 307 | 17 837 |
| No. of solvents | 8 (Lys), 4 (FAD), 4 (PEG) | 8 (Orn), 4 (FAD) | 8 (Arg), 4 (FAD) |
| RMSD from ideal values | |||
| Bond lengths (Å) | 0.017 | 0.017 | 0.015 |
| Bond angles (°) | 1.80 | 1.77 | 1.73 |
| Ramachandran plot (%) | |||
| Favored | 96.1 | 96.8 | 97.2 |
| Allowed | 3.3 | 2.7 | 2.2 |
| Outlier | 0.59 | 0.55 | 0.59 |
Values in parentheses correspond to the highest resolution shell.