Table 1.
PP method | Eluate volume (mL) | Labelling media | Buffer volume (mL) | DATATOC (nmol/μM) | Labelling pH |
---|---|---|---|---|---|
Fractionation | 0.900 | 1.00 M NH4OAc | 0.200 | 13 / 11.8 | 4.9 |
Acetone | 0.400 | 0.20 M NaOAc | 1.000 | 13 / 9.29 | 4.5 |
Ethanol | 1.000 | 1.00 M NH4OAc | 1.500 | 13 / 5.20 | 4.9 |
NaCl | 0.510 | 1.00 M NH4OAc | 3.500 | 13 / 3.24 | 4.2 |