Table 1.
PinsTPR-InscASYM | Dataset 1 | Dataset 2 |
---|---|---|
Data collection | ||
Space group | P212121 | P212121 |
Cell dimensions | ||
a, b, c (Å) | 128.19, 212.58, 280.73 | 127.08, 214.07, 279.68 |
α, β, γ (°) | 90° 90° 90° | 90° 90° 90° |
Resolution (Å) | 75.6–3.4 (3.52–3.4)* | 70.6–4.0 (4.1–4.0)* |
Rmerge | 0.2328 (1.422) | 0.3384 (1.896) |
I/σI | 12.7 (2.15) | 6.21 (1.23) |
Completeness (%) | 99.9 (99.98) | 99.8 (98.9) |
Redundancy | 14.9 (14.1) | 6.7 (7.0) |
Refinement | ||
Resolution (Å) | 75.6–3.4 | |
Reflections used | 105843 | |
Rwork/Rfree | 0.209/0.249 | |
No. atoms | 38983 | |
Protein | 38979 | |
Ligand/ion | 0 | |
Water | 4 | |
B-factors | ||
Protein | 78.0 | |
Ligand/ion | 0 | |
Water | 30 | |
R.m.s deviations | ||
Bond lengths (Å) | 0.003 | |
Bond angles (°) | 0.53 |
*Values in parentheses are for highest-resolution shell