Table 1.
Parameter | Conditions |
---|---|
Dispenser operation conditions | |
Dispensing volume | 2,000 μL |
Dispensing time | 21 s |
Dispenser temperature | 200 ºC |
Volumetric intensity of carrier gas flow | 30 mL/min |
Parameters of sorption trap operation | |
Trap temperature | 50 ºC |
Retention time | 26 s |
Conditions for chromatographic analysis | |
Temperature program | 50 ºC (2 s) - |
3 ºC/s – 250 ºC | |
(21 s) | |
Carrier gas | Hydrogen |
Dispenser temperature | 270 ºC |
Detector operation conditions | |
Detector temperature | 260 ºC |
Acquisition time | 110 s |