Table 3.
Anomalous diffraction ratios
20.0 < d < 4.0 Å
|
4.0 < d < 3.2 Å
|
Scattering factors (e)
|
||||||||
---|---|---|---|---|---|---|---|---|---|---|
λ1 | λ2 | λ3 | λ4 | λ1 | λ2 | λ3 | λ4 | f′ | f" | |
λ1 | 0.248 (0.101) | 0.145 | 0.168 | 0.144 | 0.253 (0.127) | 0.159 | 0.187 | 0.165 | −77.9 | 45.3 |
λ2 | 0.329 (0.096) | 0.115 | 0.133 | 0.323 (0.121) | 0.140 | 0.162 | −43.7 | 72.2 | ||
λ3 | 0.229 (0.093) | 0.102 | 0.247 (0.121) | 0.140 | −15.4 | 53.9 | ||||
λ4 | 0.165 (0.092) | 0.195 (0.120) | −31.0 | 32.0 |
Table values represent rms(Δ|F|)/rms(|F|), where Δ|F| is the Bijvoet difference at one wavelength (diagonal elements) or of the dispersive difference between two wavelengths (off-diagonal elements). The values in parentheses are the ratios for centric Bijvoet reflections, which would be equal to zero for perfect data; these serve as an estimate of the noise in the anomalous signals.