Table 3.
Atom # | 13C Chemical Shift, ppm | 1H Chemical Shift, ppm | # H`s | Signal Splitting |
---|---|---|---|---|
1 | 17.9 | 1.87 | 6 | singlet |
2 | 135.3 | 0 | ||
3 | 126.7 | 5.75, 6.03 | 2, 2 | singlets |
4 | 165.6 | 0 | ||
5 | 64.7 | 4.04, 4.63 | 2, 2 | doublets |
6 | 62.2 | 3.30, 3.59 | 2, 2 | multiplets |
7, 8 | 49.9, 50.0 | 2.66, 2.93 | 6, 6 | singlets |
9 | 57.6 | 4.22 | 4 | broad |
10 | 141.8 | 0 | ||
11 | 125.1 | 0 | ||
12 | 135.1 | 7.82 | 2 | multiplet |
13 | 131.0 | 7.69 | 2 | triplet |
14 | 128.4 | 7.63 | 2 | triplet |
15 | 132.8 | 7.52 | 2 | multiplet |