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. 2018 Jan 27;5(1):14. doi: 10.3390/medicines5010014

Table 1.

UV-vis and mass spectral characteristics of the main polyphenolic phytochemicals detected in the Bt extracts of S. mucronata.

Peak Rt (min) λmax (nm) [M + H]+ (m/z) Other Ions (m/z) Tentative Identity
1 16.39 298 (s), 322 779 765, 751, 731, 503, 489, 457, 355, 163 Chlorogenate derivative
2 24.68 242, 292 (s), 344 763 627, 465, 441, 393, 371, 303 Quercetin derivative
3 25.11 250, 348 449 287 Luteolin glucoside
4 26.32 278, 300 (s), 344 653 611, 287 Luteolin derivative
5 26.52 242, 374 (s), 392 669 653, 517, 303 Quercetin derivative
6 26.72 272, 300, 330 653 449 Isoscutellarein acetylallosylglucoside
7 26.88 265, 340 433 271 Apigenin C-glucoside
8 29.03 270, 304 (s), 358 653 287 Luteolin derivative
9 29.73 252, 280, 344 695 653, 287 Luteolin derivative
10 32.74 234, 336 579 447, 271 Apigenin derivative
11 33.73 264, 302 (s), 364 695 717 [M + Na]+, 287 Luteolin derivative
12 33.97 232, 276, 306, 332 695 717 [M + Na]+, 287 Luteolin derivative
13 34.35 234, 268, 316, 344 579 601 [M + Na]+, 271 Apigenin derivative