Scheme 2.
Scheme for the synthesis of ADIBO-OTs and ADIBO-F.
a) tert-butyldimethylsilyl chloride, imidazole, DMF b) TritonB, MeOH c) EDC, DMAP, N-hydroxysuccinimide, DMF d) TsF, DBU, MeCN e) TBAF, THF
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