Fig. 6. 1H NMR spectra of (a) ZnEt2 and [Zn5(Et)4(Ole)6], the hydrolysed products observed at (b) 0.53 equiv. H2O added, (c) 1.06 equiv. H2O added, (d) 1.60 equiv. H2O added and (e) the bulk LZH-Ole. *: silicon grease, #: ethane (δ 0.80 ppm), C: [Zn5(Et)4(Ole)6], L: LZH-Ole, X: ZnEt2 (δ 0.10 & δ 1.12 ppm), ‡ & †: alkenyl protons of oleate (δ 5.51 & δ 5.61 ppm).
