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Stoichiometric reaction between (tBuNC)2Pd(O2) 1 and N-methoxy-2,6-difluorobenzamide to afford the cis-bisamidate-PdII product 5F (A) and in situ IR spectra of (tBuNC)2Pd(O2) 1 and the product of the stoichiometric reaction between (tBuNC)2Pd(O2) and N-methoxy-2,6-difluorobenzamide: cis-(tBuNC)2Pd(SubF2)2 5F (B). The scaling of the absorbance of the spectrum of 5F has been magnified by a factor of 3 to account for dilution relative to the sample used for the spectrum of 1.
