Table 2.
No. | 1 a | 2 a | 3 a | 4 a | 5 a | 6 b |
---|---|---|---|---|---|---|
1 | 139.4, C | 138.0, C | 139.1, C | 137.6, C | 148.7, C | 138.1, C |
2 | 133.2, C | 133.8, C | 133.5, C | 134.1, C | 130.6, C | 130.0, C |
3 | 42.4, CH | 46.6, CH | 42.4, CH | 46.5, CH | 39.3, CH | 41.5, CH |
4 | 37.2, CH2 | 37.1, CH2 | 37.3, CH2 | 37.2, CH2 | 34.0, CH2 | 34.5, CH2 |
5 | 178.3, C | 174.3, C | 178.3, C | 174.3, C | 180.5, C | 174.3, C |
6 | 144.2, CH | 144.5, CH | 144.0, CH | 144.3, CH | 71.4, CH | 66.3, CH |
7 | 49.3, CH | 48.7, CH | 48.3, CH | 48.8, CH | 49.2, CH | 47.9, CH |
8 | 44.4, CH2 | 44.3, CH2 | 44.1, CH2 | 44.2, CH2 | 42.5, CH2 | 39.9, CH2 |
9 | 44.6, C | 44.7, C | 44.8, C | 44.8, C | 38.4, C | 37.4, C |
10 | 42.7, CH2 | 42.6, CH2 | 42.9, CH2 | 42.6, CH2 | 46.5, CH2 | 48.5, CH2 |
11 | 70.2, CH2 | 69.4, CH2 | 70.2, CH2 | 69.5, CH2 | 60.1, CH2 | 71.5, CH2 |
12 | 110.6, CH | 102.7, CH | 110.5, CH | 102.7, CH | 73.9, CH2 | 109.8, CH |
13 | 115.0, CH2 | 114.5, CH2 | 115.1, CH2 | 114.5, CH2 | 19.4, CH3 | 20.7, CH3 |
14 | 69.2, CH2 | 69.3, CH2 | 23.1, CH3 | 23.2, CH3 | 29.6, CH3 | 27.4, CH3 |
15 | 24.5, CH3 | 24.5, CH3 | 70.9, CH2 | 71.1, CH2 | 28.6, CH3 | 28.6, CH3 |
16 | 52.3, CH3 | 52.3, CH3 |
aRecorded in CD3OD, recorded in 150 MHz
bRecorded in CDCl3, recorded in 200 MHz