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. 2018 Mar 19;8(2):113–119. doi: 10.1007/s13659-018-0157-y

Table 2.

13C NMR spectroscopic data of compounds 16 (150 MHz, δ in ppm)

No. 1 a 2 a 3 a 4 a 5 a 6 b
1 139.4, C 138.0, C 139.1, C 137.6, C 148.7, C 138.1, C
2 133.2, C 133.8, C 133.5, C 134.1, C 130.6, C 130.0, C
3 42.4, CH 46.6, CH 42.4, CH 46.5, CH 39.3, CH 41.5, CH
4 37.2, CH2 37.1, CH2 37.3, CH2 37.2, CH2 34.0, CH2 34.5, CH2
5 178.3, C 174.3, C 178.3, C 174.3, C 180.5, C 174.3, C
6 144.2, CH 144.5, CH 144.0, CH 144.3, CH 71.4, CH 66.3, CH
7 49.3, CH 48.7, CH 48.3, CH 48.8, CH 49.2, CH 47.9, CH
8 44.4, CH2 44.3, CH2 44.1, CH2 44.2, CH2 42.5, CH2 39.9, CH2
9 44.6, C 44.7, C 44.8, C 44.8, C 38.4, C 37.4, C
10 42.7, CH2 42.6, CH2 42.9, CH2 42.6, CH2 46.5, CH2 48.5, CH2
11 70.2, CH2 69.4, CH2 70.2, CH2 69.5, CH2 60.1, CH2 71.5, CH2
12 110.6, CH 102.7, CH 110.5, CH 102.7, CH 73.9, CH2 109.8, CH
13 115.0, CH2 114.5, CH2 115.1, CH2 114.5, CH2 19.4, CH3 20.7, CH3
14 69.2, CH2 69.3, CH2 23.1, CH3 23.2, CH3 29.6, CH3 27.4, CH3
15 24.5, CH3 24.5, CH3 70.9, CH2 71.1, CH2 28.6, CH3 28.6, CH3
16 52.3, CH3 52.3, CH3

aRecorded in CD3OD, recorded in 150 MHz

bRecorded in CDCl3, recorded in 200 MHz