Table 1. Crystallographic Data Collection and Refinement Statisticsa.
data collection | BAZ2A-ART | BAZ2A-ARTAATARKS | BAZ2A-Fr19 | BAZ2A-Fr23 |
---|---|---|---|---|
space group | P43212 | P43212 | P43212 | P43212 |
cell dimensions | ||||
a, b, c (Å) | 73.4, 73.4, 99.7 | 72.7, 72.7, 99.9 | 72.1, 72.1, 99.2 | 72.8, 72.8, 99.6 |
α, β, γ (deg) | 90, 90, 90 | 90, 90, 90 | 90, 90, 90 | 90, 90, 90 |
resolution | 46.03 (2.0) | 45.72 (2.0) | 45.34 (1.9) | 45.2 (2.7) |
unique observations | 19049 | 18751 | 21069 | 7841 |
completeness (%) | 99.9 (99.9) | 99.9 (99.9) | 99.3 (98.8) | 100 (100) |
redundancy | 8.6 (9.0) | 9.7 (9.9) | 3.8 (4.0) | 12 (12.3) |
CC1/2 | 0.99 (0.78) | 0.99 (0.91) | 0.99 (0.83) | 0.99 (0.95) |
I/σ(I) | 15.5 (2.1) | 14.0 (4.0) | 14.3 (2.6) | 10.7 (3.7) |
wavelength (Å) | 0.9282 | 0.9763 | 0.9763 | 0.9686 |
refinement | ||||
Rwork/Rfree (%) | 19.3/23.5 | 19.4/22.3 | 18.9/23.1 | 20.8/24.4 |
rmsd bond (Å) | 0.011 | 0.007 | 0.015 | 0.005 |
rmsd angle (deg) | 1.6 | 1.26 | 1.9 | 0.75 |
PDB code | 6FHU | 6FKP | 6FI0 | 6FAP |
data collection | BAZ2B–Fr21 | BAZ2B–Fr23 |
---|---|---|
space group | P212121 | P212121 |
cell dimensions | ||
a, b, c (Å) | 38.3, 45.4, 65.0 | 37.8, 45.5, 64.8 |
α, β, γ (deg) | 90, 90, 90 | 90, 90, 90 |
resolution | 65.04 (1.95) | 64.83 (2.7) |
unique observations | 8453 | 3349 |
completeness | 97.7 (87.1) | 100.0 (100.0) |
redundancy | 5.8 (4.9) | 5.6 (5.9) |
CC1/2 | 0.99 (0.91) | 0.96 (0.56) |
I/σ(I) | 18.1 (1.3) | 5.3 (1.9) |
wavelength (Å) | 0.9686 | 0.9686 |
refinement | ||
Rwork/Rfree (%) | 18.5/23.8 | 22.6/29.9 |
rmsd bond (Å) | 0.02 | 0.014 |
rmsd angle (deg) | 1.88 | 1.73 |
PDB code | 6FHQ | 6FI1 |
Values shown in parentheses are for the highest resolution shell.