Table 1.

Molar ratios of reaction species (TEOS = 1) with diameters obtained from dimensional measurements

Sample	EtOH	H2O	NH3	DMSO	FCPTES (× 10−4)	Avg. Ø (nm)
D0F2	86	33.2	2.4		2	32 ± 3b
D0F5	86	33.2	2.4		5	35 ± 3b
D14F2	86	33.2	2.4	14.2	2	3 ± 1b
D7F0	86	33.2	2.4	7.1		5 ± 1b (14 ± 7d)
D3F0	86	33.2	2.4	3.5		15 ± 3b (20 ± 7d)
E86	86	5.3	2.4	14.2	2	9 ± 2c
E129	129	5.3	2.4	14.2	2	13 ± 4c
E172	172	5.3	2.4	14.2	2	18 ± 5c
E215	215	5.3	2.4	14.2	2	8 ± 2c
E258	258	5.3	2.4	14.2	2	7 ± 2c
W2N1	200	2.2 (33.6a)	1		1	12 ± 4c
W4N2	200	4.4 (35.8a)	2		1	23 ± 5c
W8N4	200	8.8 (40.2a)	4		1	55 ± 8c
W17N8	200	17.6 (49.0a)	8		1	200 ± 20c
W26N12	200	26.3 (57.7a)	12		1	250 ± 25c

D7F0: PDI = 0.24; D3F0: PDI = 0.14

^aAdditional H₂O = 31.4

^bAFM

^cSEM

^dDLS