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. 2018 Mar 21;16(4):99. doi: 10.3390/md16040099

Table 1.

13C- and 1H-NMR data (150 and 600 MHz in CDCl3; δ in ppm, J in Hz) of 1 and 2.

No. 1 2
δC δH δC δH
1 40.2 (CH) 3.10 ddd (3.4, 8.3, 11.7) 39.1 (CH) 3.12 ddd (2.8, 8.3, 11.7)
2 77.6 (CH) 5.53 dd (8.3, 11.0) 77.1 (CH) 5.48 dd (8.3, 11.0)
3 119.8 (CH) 4.90 d (11.0) 120.0 (CH) 5.00 d (11.0)
4 143.8 (C) 142.4 (C)
5 39.6 (CH2) 2.16 m 43.1 (CH2) 2.78 m
1.80 dt (4.8, 12.4) 2.76 m
6 24.2 (CH2) 2.39 m 128.6 (CH) 5.80 td (8.3, 15.8)
2.03 m
7 125.6 (CH) 4.70 br d (8.9) 136.4 (CH) 5.46 d (15.8)
8 133.2 (C) 84.4 (C)
9 39.5 (CH2) 2.31 br d (13.8) 37.7 (CH2) 1.77 m
2.14 m 1.72 m
10 22.9 (CH2) 2.14 m 22.5 (CH2) 2.36 m
2.00 m 1.96 m
11 129.8 (CH) 5.23 dd (5.5, 9.6) 130.5 (C) 5.31 dd (4.1, 10.3)
12 132.0 (C) 131.9 (C)
13 77.3 (CH) 5.04 d (11.0) 76.8 (CH) 5.00 d (11.7)
14 32.4 (CH2) 2.41 m 32.6 (CH2) 2.20 ddd (2.8, 11.7, 14.4)
1.54 m 1.52 dd (11.7, 14.4)
15 138.3 (C) 138.1 (C)
16 170.3 (C) 170.2 (C)
17 120.2 (CH2) 6.25 d (3.4) 120.9 (CH2) 6.28 d (3.4)
5.49 d (3.4) 5.52 d (3.4)
18 15.1 (CH3) 1.75 s 16.1 (CH3) 1.91 s
19 15.2 (CH3) 1.58 s 20.7 (CH3) 1.42 s
20 10.2 (CH3) 1.60 s 10.2 (CH3) 1.61 s
13-OAc 170.9 (C) 170.9 (C)
21.2 (CH3) 2.05 s 21.2 (CH3) 2.05 s