Table 1.
Data collection | |
---|---|
Wavelength (Å) | 0.9802 |
Resolution range (Å) | 62.88–2.65 (2.745–2.65) |
Space group | P21212 |
Cell dimensions: a, b, c (Å) | 255.31, 64.88, 144.72 |
Total reflections | 2,860,846 (70,986) |
Unique reflections | 70,861 (6900) |
Multiplicity | 40.4 (10.3) |
Completeness (%) | 99.84 (98.94) |
Mean I/sigma(I) | 17.42 (0.86) |
Wilson B-factor | 86.41 |
Rmeas | 0.167 (4.17) |
CC1/2 | 0.999 (0.611) |
Refinement | |
Rwork (%) | 23.54 (36.96) |
Rfree (%) | 26.04 (42.30) |
Non-hydrogen atoms (protein/glycan) | 13,132/53 |
Bonds lengths (Å) | 0.002 |
Angles (°) | 0.52 |
Ramachandran favoured/outliers (%) | 96.68/0.0 |
Clash score | 4.30 |
Average B-factor | 113.91 |