Table 1.
Data collection and refinement statistics
Rmeas = Σhkl(N/(N − 1))½Σi|Ii(hkl) − I(hkl)|/ΣhklΣiIi(hkl). CC½ is the correlation between random half-data sets. The statistics for the highest-resolution shell are shown in parentheses.
| Data collection | |
|---|---|
| Wavelength (Å) | 0.9802 |
| Resolution range (Å) | 62.88–2.65 (2.745–2.65) |
| Space group | P21212 |
| Cell dimensions: a, b, c (Å) | 255.31, 64.88, 144.72 |
| Total reflections | 2,860,846 (70,986) |
| Unique reflections | 70,861 (6900) |
| Multiplicity | 40.4 (10.3) |
| Completeness (%) | 99.84 (98.94) |
| Mean I/sigma(I) | 17.42 (0.86) |
| Wilson B-factor | 86.41 |
| Rmeas | 0.167 (4.17) |
| CC1/2 | 0.999 (0.611) |
| Refinement | |
| Rwork (%) | 23.54 (36.96) |
| Rfree (%) | 26.04 (42.30) |
| Non-hydrogen atoms (protein/glycan) | 13,132/53 |
| Bonds lengths (Å) | 0.002 |
| Angles (°) | 0.52 |
| Ramachandran favoured/outliers (%) | 96.68/0.0 |
| Clash score | 4.30 |
| Average B-factor | 113.91 |