Table 1.
Main parameters of the hydrolysis process and range of values investigated.
Step | Parameter | Range |
---|---|---|
Pre-treatment | Mass ratio of sulfuric acid/dry cellulose (R1) | 12–36 |
Mass percentage of sulfuric acid (C1) | 62–82 wt% | |
Time (t1) | 0–2 h | |
Partial neutralization | Acid/base molar ratio (R2) | 1–3 |
Concentration of base (C2) | 29 wt% NH3(aq) | |
20–40 wt% NaOH | ||
Post-hydrolysis | Time (t2) | 0–3 h |
Temperature (T1) | 97–121°C |