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. 2018 May 3;74(Pt 3):170–183. doi: 10.1107/S2053273318004308

Table 1. Crystal data and diffraction data collection statistics for the BOH2 molecule.

Crystal data  
Chemical formula C11H15BO2
Molecular weight 190.039
Crystal system, space group Orthorhombic, Pbca
Temperature (K) 90 (1)
a, b, c (Å) 7.52004(9), 9.38374 (13), 30.7120 (5)
Volume (Å3), Z 2167.23 (5), 8
Radiation type Mo Kα
λ (Å) 0.71073
F (000) 816
Crystal shape and colour Block and colourless
Crystal dimensions (mm) 0.34 × 0.18 × 0.10
Data collection  
Diffractometer Rigaku MicroMax-007HF
Absorption correction CrysAlisPro 1.171.38.37f
Absorption coefficient μ (mm−1) 0.077
Inline graphic 0.472, 0.999
sinθmax/λ (Å−1) 1.12
No. measured, unique reflections 117 942, 12 055
No. reflections (I > 2σ) 10 680
Completeness (%) at sinθmax 96.5
R int 3.06%
Refinement  
Weighting scheme W hkl = 3.3/σI 2
wR 2(I), R(F) 3.62%, 2.70%
Goodness of fit 1.0

Rigaku Oxford Diffraction (2015).

At sinθmax/λ = 1.22 Å−1.