Table 1. Data collection and refinement statistics.
| TnpA/LE29/T6′ | |
|---|---|
| Crystal properties | |
| Space group | P41212 |
| Unit cell: a, b, c (Å) | 138.64, 138.64, 117.95 |
| Unit cell: α, β, γ (°) | 90, 90, 90 |
| Data collection | |
| Beamline | ID30B (ESRF) |
| Wavelength (Å) | 0.97 |
| Resolution range (Å) | 89.84–2.6 (2.691–2.598) |
| Total reflections | 351387 (35340) |
| Unique reflections | 35947 (3525) |
| Multiplicity | 9.8 (10.0) |
| Completeness (%) | 99.72 (99.58) |
| R-merge | 0.2929 (1.317) |
| R-meas | 0.3091 (1.387) |
| R-pim | 0.09723 (0.4295) |
| I/σI | 6.03 (1.40) |
| CC1/2 | 0.994 (0.738) |
| Wilson B-factor | 38.49 |
| Refinement | |
| R-work | 0.1970 (0.3030) |
| R-free | 0.2383 (0.3609) |
| Number of non-hydrogen atoms | 7412 |
| Protein residues | 508 |
| RMS (bonds) | 0.003 |
| RMS (angles) | 0.57 |
| Ramachandran favoured (%) | 97.20 |
| Ramachandran outliers (%) | 0.00 |
| Clashscore | 2.63 |
| Average B-factor | 34.98 |
| Number of TLS groups | 12 |
Values in parentheses refer to the highest resolution shell.