. Author manuscript; available in PMC: 2018 May 7.

Published in final edited form as: Acta Crystallogr D Struct Biol. 2016 Jul 27;72(Pt 8):944–955. doi: 10.1107/S2059798316010834

Table 1.

Data collection and processing

Diffraction source	LCLS XFEL source (XPP Endstation)
Wavelength (Å)	1.29
Temperature (K)	293
Detector	Rayonix MX170-HS CCD
Crystal-detector distance (mm)	340
Exposure time per image (s)	0.1
Space group	P21 21 21
a, b, c (Å)	38.13, 46.48, 84.52
α, β, γ (°)	90.00, 90.00, 90.00
Resolution range (Å)	33.43-1.9
Images merged	8957
No. of unique reflections	12354
Completeness (%)	100
〈I/σ(I)〉	6.0
Multiplicity	51.6
Rsplit(%)	10.1(46.1)
Matthew’s coefficient, V_M (Å³/Da)	2.18
Solvent content, Vs (%)	43.5
Observations per image to edge of detector	166 ± 28
CC1/2 (%)	99.6 (42.6)